TY - JOUR
T1 - 1,4,7-triazacyclononane hemihydrate
AU - Battle, Andrew R.
AU - Johnson, Daniel L.
AU - Martin, Lisandra L.
PY - 2005/2
Y1 - 2005/2
N2 - The title compound, C6H15N 3·0.5H2O, crystallizes in the high-symmetry trigonal space group P3c1. This is, after more than 30 years of effort on this compound, the first reported structure of the free base of this macrocycle. Six N-H⋯O hydrogen bonds are formed between the water O atom occupying a special site at the origin and N atoms of six neighbouring 1,4,7-triazacyclononane molecules.
AB - The title compound, C6H15N 3·0.5H2O, crystallizes in the high-symmetry trigonal space group P3c1. This is, after more than 30 years of effort on this compound, the first reported structure of the free base of this macrocycle. Six N-H⋯O hydrogen bonds are formed between the water O atom occupying a special site at the origin and N atoms of six neighbouring 1,4,7-triazacyclononane molecules.
UR - http://www.scopus.com/inward/record.url?scp=18544378876&partnerID=8YFLogxK
U2 - 10.1107/S1600536805000814
DO - 10.1107/S1600536805000814
M3 - Article
AN - SCOPUS:18544378876
VL - 61
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
SN - 1600-5368
IS - 2
ER -