A beamline for high-pressure studies at the advanced light source with a superconducting bending magnet as the source

Martin Kunz; Alastair A. MacDowell; Wendel A. Caldwell; Daniella Cambie; Richard S. Celestre; Edward E. Domning; Robert M. Duarte; Arianna E. Gleason; James M. Glossinger; Nicholas Kelez; David W. Plate; Tony Yu; Joeseph M. Zaug; Howard A. Padmore; Raymond Jeanloz; A. Paul Alivisatos; Simon M. Clark

doi:10.1107/S0909049505020959

A beamline for high-pressure studies at the advanced light source with a superconducting bending magnet as the source

Martin Kunz^*, Alastair A. MacDowell, Wendel A. Caldwell, Daniella Cambie, Richard S. Celestre, Edward E. Domning, Robert M. Duarte, Arianna E. Gleason, James M. Glossinger, Nicholas Kelez, David W. Plate, Tony Yu, Joeseph M. Zaug, Howard A. Padmore, Raymond Jeanloz, A. Paul Alivisatos, Simon M. Clark

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

148 Citations (Scopus)

Abstract

A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 T superconducting bending magnet (superbend). Useful X-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness-preserving optics of the beamline. These optics are comprised of a plane parabola collimating mirror, followed by a Kohzu monochromator vessel with Si(111) crystals (E/ΔE ≃ 7000) and W/B₄C multilayers (E/ΔE ≃ 100), and then a toroidal focusing mirror with variable focusing distance. The experimental enclosure contains an automated beam-positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detector (CCD or image-plate detector). Future developments aim at the installation of a second endstation dedicated to in situ laser heating and a dedicated high-pressure single-crystal station, applying both monochromatic and polychromatic techniques.

Original language	English
Pages (from-to)	650-658
Number of pages	9
Journal	Journal of Synchrotron Radiation
Volume	12
Issue number	5
DOIs	https://doi.org/10.1107/S0909049505020959
Publication status	Published - Sept 2005
Externally published	Yes

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Kunz, M., MacDowell, A. A., Caldwell, W. A., Cambie, D., Celestre, R. S., Domning, E. E., Duarte, R. M., Gleason, A. E., Glossinger, J. M., Kelez, N., Plate, D. W., Yu, T., Zaug, J. M., Padmore, H. A., Jeanloz, R., Alivisatos, A. P., & Clark, S. M. (2005). A beamline for high-pressure studies at the advanced light source with a superconducting bending magnet as the source. Journal of Synchrotron Radiation, 12(5), 650-658. https://doi.org/10.1107/S0909049505020959

@article{90e09b95b2b94fbe8cd9551dc5c530bb,

title = "A beamline for high-pressure studies at the advanced light source with a superconducting bending magnet as the source",

abstract = "A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 T superconducting bending magnet (superbend). Useful X-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness-preserving optics of the beamline. These optics are comprised of a plane parabola collimating mirror, followed by a Kohzu monochromator vessel with Si(111) crystals (E/ΔE ≃ 7000) and W/B4C multilayers (E/ΔE ≃ 100), and then a toroidal focusing mirror with variable focusing distance. The experimental enclosure contains an automated beam-positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detector (CCD or image-plate detector). Future developments aim at the installation of a second endstation dedicated to in situ laser heating and a dedicated high-pressure single-crystal station, applying both monochromatic and polychromatic techniques.",

author = "Martin Kunz and MacDowell, {Alastair A.} and Caldwell, {Wendel A.} and Daniella Cambie and Celestre, {Richard S.} and Domning, {Edward E.} and Duarte, {Robert M.} and Gleason, {Arianna E.} and Glossinger, {James M.} and Nicholas Kelez and Plate, {David W.} and Tony Yu and Zaug, {Joeseph M.} and Padmore, {Howard A.} and Raymond Jeanloz and Alivisatos, {A. Paul} and Clark, {Simon M.}",

year = "2005",

month = sep,

doi = "10.1107/S0909049505020959",

language = "English",

volume = "12",

pages = "650--658",

journal = "Journal of Synchrotron Radiation",

issn = "0909-0495",

publisher = "International Union of Crystallography",

number = "5",

}

Kunz, M, MacDowell, AA, Caldwell, WA, Cambie, D, Celestre, RS, Domning, EE, Duarte, RM, Gleason, AE, Glossinger, JM, Kelez, N, Plate, DW, Yu, T, Zaug, JM, Padmore, HA, Jeanloz, R, Alivisatos, AP & Clark, SM 2005, 'A beamline for high-pressure studies at the advanced light source with a superconducting bending magnet as the source', Journal of Synchrotron Radiation, vol. 12, no. 5, pp. 650-658. https://doi.org/10.1107/S0909049505020959

TY - JOUR

T1 - A beamline for high-pressure studies at the advanced light source with a superconducting bending magnet as the source

AU - Kunz, Martin

AU - MacDowell, Alastair A.

AU - Caldwell, Wendel A.

AU - Cambie, Daniella

AU - Celestre, Richard S.

AU - Domning, Edward E.

AU - Duarte, Robert M.

AU - Gleason, Arianna E.

AU - Glossinger, James M.

AU - Kelez, Nicholas

AU - Plate, David W.

AU - Yu, Tony

AU - Zaug, Joeseph M.

AU - Padmore, Howard A.

AU - Jeanloz, Raymond

AU - Alivisatos, A. Paul

AU - Clark, Simon M.

PY - 2005/9

Y1 - 2005/9

N2 - A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 T superconducting bending magnet (superbend). Useful X-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness-preserving optics of the beamline. These optics are comprised of a plane parabola collimating mirror, followed by a Kohzu monochromator vessel with Si(111) crystals (E/ΔE ≃ 7000) and W/B4C multilayers (E/ΔE ≃ 100), and then a toroidal focusing mirror with variable focusing distance. The experimental enclosure contains an automated beam-positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detector (CCD or image-plate detector). Future developments aim at the installation of a second endstation dedicated to in situ laser heating and a dedicated high-pressure single-crystal station, applying both monochromatic and polychromatic techniques.

AB - A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 T superconducting bending magnet (superbend). Useful X-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness-preserving optics of the beamline. These optics are comprised of a plane parabola collimating mirror, followed by a Kohzu monochromator vessel with Si(111) crystals (E/ΔE ≃ 7000) and W/B4C multilayers (E/ΔE ≃ 100), and then a toroidal focusing mirror with variable focusing distance. The experimental enclosure contains an automated beam-positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detector (CCD or image-plate detector). Future developments aim at the installation of a second endstation dedicated to in situ laser heating and a dedicated high-pressure single-crystal station, applying both monochromatic and polychromatic techniques.

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DO - 10.1107/S0909049505020959

M3 - Article

C2 - 16120990

AN - SCOPUS:27644432183

SN - 0909-0495

VL - 12

SP - 650

EP - 658

JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

IS - 5

ER -

A beamline for high-pressure studies at the advanced light source with a superconducting bending magnet as the source

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