A furnace for in situ synchrotron Laue diffraction and its application to studies of solid-state phase Transformations

H. L. Bhat; S. M. Clark; A. El Korashy; K. J. Roberts

doi:10.1107/S0021889890007257

A furnace for in situ synchrotron Laue diffraction and its application to studies of solid-state phase Transformations

H. L. Bhat, S. M. Clark, A. El Korashy, K. J. Roberts

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Abstract

The design of a new microfurnace for use for Laue diffraction studies of solid-state transformations is described. The furnace operates in the temperature range 298-573 K with a thermal stability of about ± 0.1 K. The potential of the synchrotron-radiation Laue diffraction technique for studies of structural phase transitions is demonstrated. Experimental data on phase transitions in caesium periodate, potassium tetrachlorozincate and pentaerythritol are presented.

Original language	English
Pages (from-to)	545-549
Number of pages	5
Journal	Journal of Applied Crystallography
Volume	23
Issue number	6
DOIs	https://doi.org/10.1107/S0021889890007257
Publication status	Published - 1990
Externally published	Yes

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abstract = "The design of a new microfurnace for use for Laue diffraction studies of solid-state transformations is described. The furnace operates in the temperature range 298-573 K with a thermal stability of about ± 0.1 K. The potential of the synchrotron-radiation Laue diffraction technique for studies of structural phase transitions is demonstrated. Experimental data on phase transitions in caesium periodate, potassium tetrachlorozincate and pentaerythritol are presented.",

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AU - El Korashy, A.

AU - Roberts, K. J.

PY - 1990

Y1 - 1990

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AB - The design of a new microfurnace for use for Laue diffraction studies of solid-state transformations is described. The furnace operates in the temperature range 298-573 K with a thermal stability of about ± 0.1 K. The potential of the synchrotron-radiation Laue diffraction technique for studies of structural phase transitions is demonstrated. Experimental data on phase transitions in caesium periodate, potassium tetrachlorozincate and pentaerythritol are presented.

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ER -

A furnace for in situ synchrotron Laue diffraction and its application to studies of solid-state phase Transformations

Abstract

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