An apparatus for the study of the kinetics and mechanism of hydrothermal reactions by in situ energy dispersive x-ray diffraction

J. S. O. Evans; R. J. Francis; D. O'Hare; S. J. Price; S. M. Clark; J. Flaherty; J. Gordon; A. Nield; C. C. Tang

doi:10.1063/1.1146451

An apparatus for the study of the kinetics and mechanism of hydrothermal reactions by in situ energy dispersive x-ray diffraction

J. S. O. Evans, R. J. Francis, D. O'Hare, S. J. Price, S. M. Clark, J. Flaherty, J. Gordon, A. Nield, C. C. Tang

Research output: Contribution to journal › Article › peer-review

91 Citations (Scopus)

Abstract

The design and implementation of a pressure cell for the study of hydrothermal reactions by in situ energy dispersive x-ray diffraction is described. The cell permits the study of both the kinetics and mechanism of formation of a wide range of important solid-state compounds such as zeolites and other microporous solids. Reactions can be studied over a wide range of temperature (5-230 °C) and autogenous pressure [0-400 psi (gauge)] conditions. The use of this apparatus is illustrated by a study on the synthesis of a microporous tin chalcogenide phase performed on Station 9.7 of the UK Synchrotron Radiation Source.

Original language	English
Pages (from-to)	2442-2445
Number of pages	4
Journal	Review of Scientific Instruments
Volume	66
Issue number	3
DOIs	https://doi.org/10.1063/1.1146451
Publication status	Published - 1995
Externally published	Yes

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title = "An apparatus for the study of the kinetics and mechanism of hydrothermal reactions by in situ energy dispersive x-ray diffraction",

abstract = "The design and implementation of a pressure cell for the study of hydrothermal reactions by in situ energy dispersive x-ray diffraction is described. The cell permits the study of both the kinetics and mechanism of formation of a wide range of important solid-state compounds such as zeolites and other microporous solids. Reactions can be studied over a wide range of temperature (5-230 °C) and autogenous pressure [0-400 psi (gauge)] conditions. The use of this apparatus is illustrated by a study on the synthesis of a microporous tin chalcogenide phase performed on Station 9.7 of the UK Synchrotron Radiation Source.",

author = "Evans, {J. S. O.} and Francis, {R. J.} and D. O'Hare and Price, {S. J.} and Clark, {S. M.} and J. Flaherty and J. Gordon and A. Nield and Tang, {C. C.}",

year = "1995",

doi = "10.1063/1.1146451",

language = "English",

volume = "66",

pages = "2442--2445",

journal = "Review of Scientific Instruments",

issn = "0034-6748",

publisher = "American Institute of Physics",

number = "3",

}

An apparatus for the study of the kinetics and mechanism of hydrothermal reactions by in situ energy dispersive x-ray diffraction. / Evans, J. S. O.; Francis, R. J.; O'Hare, D.; Price, S. J.; Clark, S. M.; Flaherty, J.; Gordon, J.; Nield, A.; Tang, C. C.

In: Review of Scientific Instruments, Vol. 66, No. 3, 1995, p. 2442-2445.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - An apparatus for the study of the kinetics and mechanism of hydrothermal reactions by in situ energy dispersive x-ray diffraction

AU - Evans, J. S. O.

AU - Francis, R. J.

AU - O'Hare, D.

AU - Price, S. J.

AU - Clark, S. M.

AU - Flaherty, J.

AU - Gordon, J.

AU - Nield, A.

AU - Tang, C. C.

PY - 1995

Y1 - 1995

N2 - The design and implementation of a pressure cell for the study of hydrothermal reactions by in situ energy dispersive x-ray diffraction is described. The cell permits the study of both the kinetics and mechanism of formation of a wide range of important solid-state compounds such as zeolites and other microporous solids. Reactions can be studied over a wide range of temperature (5-230 °C) and autogenous pressure [0-400 psi (gauge)] conditions. The use of this apparatus is illustrated by a study on the synthesis of a microporous tin chalcogenide phase performed on Station 9.7 of the UK Synchrotron Radiation Source.

AB - The design and implementation of a pressure cell for the study of hydrothermal reactions by in situ energy dispersive x-ray diffraction is described. The cell permits the study of both the kinetics and mechanism of formation of a wide range of important solid-state compounds such as zeolites and other microporous solids. Reactions can be studied over a wide range of temperature (5-230 °C) and autogenous pressure [0-400 psi (gauge)] conditions. The use of this apparatus is illustrated by a study on the synthesis of a microporous tin chalcogenide phase performed on Station 9.7 of the UK Synchrotron Radiation Source.

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JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

SN - 0034-6748

IS - 3

ER -

An apparatus for the study of the kinetics and mechanism of hydrothermal reactions by in situ energy dispersive x-ray diffraction

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