气相色谱法测定费托合成油中的含氧化合物

Translated title of the contribution: Analysis of oxygenates in Fischer-Tropsch synthesis oil by GC

Sheng-shen Gu, Qiang-feng Yin, Jia-hui Gu, Zhong Xin*

*Corresponding author for this work

Research output: Contribution to journalArticle

Abstract

Fischer-Tropsch synthesis oil is pretreated by extracting the oxygenates into the extraction phase. Qualitative analysis of the oxygenates and low carbon n-alcohols(C3-C10) is carried out by GC-MS and GC-FID, respectively. The qualitative results of 86 oxygenates and low carbon n-alcohols are obtained. Under the experimental conditions, the calibration curves of low carbon n-alcohol are linear in the range of 0.10 - 15.00 mL. The method recoveries are 80%-92%, with the relative standard deviation lower than 4%. The analysis results can provide basic data for catalysts and kinetics studies in the process of Fischer-Tropsch synthesis.

Translated title of the contributionAnalysis of oxygenates in Fischer-Tropsch synthesis oil by GC
Original languageChinese
Pages (from-to)197-200
Number of pages4
JournalXiandai Huagong/Modern Chemical Industry
Volume36
Issue number7
Publication statusPublished - Jul 2016
Externally publishedYes

Keywords

  • Fischer-Tropsch synthesis oil
  • gas chromatography (GC)
  • mass spectrometry (MS)
  • oxygenates
  • low carbon n-alcohols

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