Apparatus for the in situ kinetic study of reactions involving air sensitive materials using energy-dispersive powder diffraction

S. M. Clark; P. Irvin; J. Flaherty; T. Rathbone; H. V. Wong; J. S. O. Evans; D. O'Hare

doi:10.1063/1.1144729

Apparatus for the in situ kinetic study of reactions involving air sensitive materials using energy-dispersive powder diffraction

S. M. Clark^*, P. Irvin, J. Flaherty, T. Rathbone, H. V. Wong, J. S. O. Evans, D. O'Hare

^*Corresponding author for this work

Research output: Contribution to journal › Article

21 Citations (Scopus)

Abstract

A novel sample chamber has been developed for the study of chemical reactions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic reactant dispensing system, heating jacket, stirrer, and gas purge system. The use of this apparatus is illustrated with data collected on station 9.7 of the UK Synchrotron Radiation Source during a study on the intercalation of cobaltocene into tin disulfide.

Original language	English
Pages (from-to)	2210-2213
Number of pages	4
Journal	Review of Scientific Instruments
Volume	65
Issue number	7
DOIs	https://doi.org/10.1063/1.1144729
Publication status	Published - 1994
Externally published	Yes

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abstract = "A novel sample chamber has been developed for the study of chemical reactions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic reactant dispensing system, heating jacket, stirrer, and gas purge system. The use of this apparatus is illustrated with data collected on station 9.7 of the UK Synchrotron Radiation Source during a study on the intercalation of cobaltocene into tin disulfide.",

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AU - Wong, H. V.

AU - Evans, J. S. O.

AU - O'Hare, D.

PY - 1994

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AB - A novel sample chamber has been developed for the study of chemical reactions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic reactant dispensing system, heating jacket, stirrer, and gas purge system. The use of this apparatus is illustrated with data collected on station 9.7 of the UK Synchrotron Radiation Source during a study on the intercalation of cobaltocene into tin disulfide.

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