Apparatus for the in situ kinetic study of reactions involving air sensitive materials using energy-dispersive powder diffraction

S. M. Clark*, P. Irvin, J. Flaherty, T. Rathbone, H. V. Wong, J. S. O. Evans, D. O'Hare

*Corresponding author for this work

Research output: Contribution to journalArticle

21 Citations (Scopus)

Abstract

A novel sample chamber has been developed for the study of chemical reactions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic reactant dispensing system, heating jacket, stirrer, and gas purge system. The use of this apparatus is illustrated with data collected on station 9.7 of the UK Synchrotron Radiation Source during a study on the intercalation of cobaltocene into tin disulfide.

Original languageEnglish
Pages (from-to)2210-2213
Number of pages4
JournalReview of Scientific Instruments
Volume65
Issue number7
DOIs
Publication statusPublished - 1994
Externally publishedYes

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