Two novel sample chambers for the energy-dispersive powder diffraction study of chemical reactions are presented. One for air sensitive samples and the other for hydrothermal synthesis. The use of these vessels is illustrated with data collected during a study of the intercalation of cobaltocene into SnS2.
|Number of pages||4|
|Journal||Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms|
|Publication status||Published - 2 May 1995|