Abstract
In order to generate homogeneous high temperatures at high pressures, a ring-shaped graphite heater has been developed to resistively heat diamond-anvil cell (DAC) samples up to 1300 K. By putting the heater in direct contact with the diamond anvils, this graphite heater design features the following advantages: (1) efficient heating: sample can be heated to 1300 K while the DAC body temperature remains less than 800 K, eliminating the requirement of a special alloy for the DAC; (2) compact design: the sample can be analyzed with in situ measurements, e.g., x-ray, optical, and electrical probes are possible. In particular, the side access of the heater allows for radial x-ray diffraction (XRD) measurements in addition to traditional axial XRD.
Original language | English |
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Pages (from-to) | 024502-1-024502-5 |
Number of pages | 5 |
Journal | Review of Scientific Instruments |
Volume | 84 |
Issue number | 2 |
DOIs | |
Publication status | Published - 2013 |
Externally published | Yes |