Following the crystallization of microporous solids using EDXRD techniques

Andrew T. Davies; Gopinathan Sankar; C. Richard A Catlow; Simon M. Clark

Following the crystallization of microporous solids using EDXRD techniques

Andrew T. Davies, Gopinathan Sankar^*, C. Richard A Catlow, Simon M. Clark

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

64 Citations (Scopus)

Abstract

Energy dispersive X-ray diffraction (EDXRD) techniques are applied to study the development of crystalline phases during the synthesis of microporous materials. We present data for both zeolite A and AlPO-5 systems. We explore the effects of template concentration and of temperature. The measured activation energy for zeolite A of ∼58 kJ mol^-1 accords well with that observed for other silicate systems. The kinetics revealed by our study accord with the nucleation/growth model of the Avrami-Erofeev treatment.

Original language	English
Pages (from-to)	10115-10120
Number of pages	6
Journal	Journal of Physical Chemistry B
Volume	101
Issue number	48
Publication status	Published - 27 Nov 1997
Externally published	Yes

Cite this

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title = "Following the crystallization of microporous solids using EDXRD techniques",

abstract = "Energy dispersive X-ray diffraction (EDXRD) techniques are applied to study the development of crystalline phases during the synthesis of microporous materials. We present data for both zeolite A and AlPO-5 systems. We explore the effects of template concentration and of temperature. The measured activation energy for zeolite A of ∼58 kJ mol-1 accords well with that observed for other silicate systems. The kinetics revealed by our study accord with the nucleation/growth model of the Avrami-Erofeev treatment.",

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AU - Davies, Andrew T.

AU - Sankar, Gopinathan

AU - Catlow, C. Richard A

AU - Clark, Simon M.

PY - 1997/11/27

Y1 - 1997/11/27

N2 - Energy dispersive X-ray diffraction (EDXRD) techniques are applied to study the development of crystalline phases during the synthesis of microporous materials. We present data for both zeolite A and AlPO-5 systems. We explore the effects of template concentration and of temperature. The measured activation energy for zeolite A of ∼58 kJ mol-1 accords well with that observed for other silicate systems. The kinetics revealed by our study accord with the nucleation/growth model of the Avrami-Erofeev treatment.

AB - Energy dispersive X-ray diffraction (EDXRD) techniques are applied to study the development of crystalline phases during the synthesis of microporous materials. We present data for both zeolite A and AlPO-5 systems. We explore the effects of template concentration and of temperature. The measured activation energy for zeolite A of ∼58 kJ mol-1 accords well with that observed for other silicate systems. The kinetics revealed by our study accord with the nucleation/growth model of the Avrami-Erofeev treatment.

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M3 - Article

AN - SCOPUS:0031269637

SN - 1089-5647

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EP - 10120

JO - Journal of Physical Chemistry B

JF - Journal of Physical Chemistry B

IS - 48

ER -

Following the crystallization of microporous solids using EDXRD techniques

Abstract

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