Formation of silica-surfactant mesophases studied by real-time in situ X-ray powder diffraction

Stephen O'Brien; Robin J. Francis; Stephen J. Price; Dermot O'Hare; Simon M. Clark; Nanae Okazaki; Kazuyuki Kuroda

doi:10.1039/C39950002423

Formation of silica-surfactant mesophases studied by real-time in situ X-ray powder diffraction

Stephen O'Brien, Robin J. Francis, Stephen J. Price, Dermot O'Hare^*, Simon M. Clark, Nanae Okazaki, Kazuyuki Kuroda

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

50 Citations (Scopus)

Abstract

Real-time in situ energy dispersive synchrotron X-ray powder diffraction data provides evidence for the formation of an intermediate lamellar silica-surfactant intercalate during the synthesis of the hexagonal mesophase derived from the layered polysilicate kanemite, whereas no intermediate phases are observed during the formation of the silica-surfactant mesophase that leads to the mesoporous material MCM-41.

Original language	English
Pages (from-to)	2423-2424
Number of pages	2
Journal	Journal of the Chemical Society, Chemical Communications
Issue number	23
DOIs	https://doi.org/10.1039/C39950002423
Publication status	Published - 1995
Externally published	Yes

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10.1039/C39950002423

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title = "Formation of silica-surfactant mesophases studied by real-time in situ X-ray powder diffraction",

abstract = "Real-time in situ energy dispersive synchrotron X-ray powder diffraction data provides evidence for the formation of an intermediate lamellar silica-surfactant intercalate during the synthesis of the hexagonal mesophase derived from the layered polysilicate kanemite, whereas no intermediate phases are observed during the formation of the silica-surfactant mesophase that leads to the mesoporous material MCM-41.",

author = "Stephen O'Brien and Francis, {Robin J.} and Price, {Stephen J.} and Dermot O'Hare and Clark, {Simon M.} and Nanae Okazaki and Kazuyuki Kuroda",

year = "1995",

doi = "10.1039/C39950002423",

language = "English",

pages = "2423--2424",

journal = "Journal of the Chemical Society, Chemical Communications",

issn = "0022-4936",

publisher = "Chemical Society",

number = "23",

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TY - JOUR

T1 - Formation of silica-surfactant mesophases studied by real-time in situ X-ray powder diffraction

AU - O'Brien, Stephen

AU - Francis, Robin J.

AU - Price, Stephen J.

AU - O'Hare, Dermot

AU - Clark, Simon M.

AU - Okazaki, Nanae

AU - Kuroda, Kazuyuki

PY - 1995

Y1 - 1995

N2 - Real-time in situ energy dispersive synchrotron X-ray powder diffraction data provides evidence for the formation of an intermediate lamellar silica-surfactant intercalate during the synthesis of the hexagonal mesophase derived from the layered polysilicate kanemite, whereas no intermediate phases are observed during the formation of the silica-surfactant mesophase that leads to the mesoporous material MCM-41.

AB - Real-time in situ energy dispersive synchrotron X-ray powder diffraction data provides evidence for the formation of an intermediate lamellar silica-surfactant intercalate during the synthesis of the hexagonal mesophase derived from the layered polysilicate kanemite, whereas no intermediate phases are observed during the formation of the silica-surfactant mesophase that leads to the mesoporous material MCM-41.

UR - http://www.scopus.com/inward/record.url?scp=37049069697&partnerID=8YFLogxK

U2 - 10.1039/C39950002423

DO - 10.1039/C39950002423

M3 - Article

AN - SCOPUS:37049069697

SN - 0022-4936

SP - 2423

EP - 2424

JO - Journal of the Chemical Society, Chemical Communications

JF - Journal of the Chemical Society, Chemical Communications

IS - 23

ER -

Formation of silica-surfactant mesophases studied by real-time in situ X-ray powder diffraction

Abstract

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