Abstract
目的:建立同时测定冠脉康片中橙皮苷和芍药苷含量的方法。方法:采用HPLC法,色谱柱为C18色谱柱(250 mm×4.6 mm,5μm),柱温25℃,以乙腈-4%醋酸(25∶80)为流动相,流速为1.0 mL/min,检测波长为230nm。结果:芍药苷进样量在0.36~5.76μg(r=0.9997)范围内,橙皮苷进样量在0.006~0.096μg(r=0.9996)范围内呈良好的线性关系,平均回收率分别为97.4%和97.0%,RSD分别为1.09%(n=6)和1.21%(n=6)。结论:该方法简单,结果准确,重现性好,可用于该制剂的质量控制。
| Translated title of the contribution | Simultaneous Determination of Paeoniflorin and Hiesperidin in Guanmaikang Tablet by HPLC |
|---|---|
| Original language | Chinese (Simplified) |
| Pages (from-to) | 53-55 |
| Number of pages | 3 |
| Journal | Journal of Liaoning University of Traditional Chinese Medicine |
| Volume | 2013 |
| Issue number | 8 |
| Publication status | Published - 2013 |
| Externally published | Yes |
Keywords
- 冠脉康片
- 芍药苷
- 橙皮苷
- HPLC
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