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Nanoscale Characterization and Imaging Techniques for Material Analysis

P. Ramshankar*, Eric Howard, Vellayan Srinivasan, D. Prabu, Joshuva Arockia Dhanraj, M. Jogendra Kumar, M. Rajendiran

*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceedingConference proceeding contributionpeer-review

Abstract

The importance of scanning electron microscopy (SEM) in nanotechnology is discussed, with a focus on its application to the study of the dynamics of nanoparticle aggregation. SEM's versatility and usefulness in fields such as environmental microscopy, voltage imaging, and biomaterial analysis have earned it great praise. With an emphasis on disentangling the complexities of nanoparticle clustering, this paper highlights the expanding potential of nanomaterials across many areas and their applications. It highlights how SEM helps characterise nanomaterials' dimensions, shapes, and surface structures, and how variables like particle concentration and surface charge affect nanoparticle stability. Nanoparticle aggregation is discussed with the use of fractal theory and molecular dynamics simulations. Different sample preparation methods for SEM analysis are addressed, along with their benefits and drawbacks. The use of SEM, and more specifically wet scanning electron microscopy, for collecting pictures of nanoparticle clusters is also highlighted. Quantitative analytic techniques are highlighted for their significance in evaluating nanoparticle size distribution and concentration, and a short comparison between scanning electron microscopy (SEM) and transmission electron microscopy (TEM) is offered. The necessity to understand these dynamics for the secure development of nanomaterials is highlighted by the fact that nanoparticle aggregation dynamics are complicated and may have ramifications for nanomaterial characteristics and applications. In conclusion, despite difficulties like sedimentation and agglomeration, SEM is positioned as a crucial instrument for researching the dynamics of nanoparticle aggregation. The text hints that fresh SEM-based approaches for sizing nanoparticles and detecting their aggregation state may be developed in future studies.

Original languageEnglish
Title of host publicationICMSA24
Subtitle of host publicationProceedings of the 5th International Conference on Material Science and Applications
Place of PublicationTamilnadu, India
PublisherAIP Publishing
Pages020023-1-020023-5
Number of pages5
ISBN (Electronic)9780735452220
DOIs
Publication statusPublished - 30 Jul 2025
Event5th International Conference on Material Science and Applications, ICMSA 2024 - Ariyalur, India
Duration: 10 Apr 202411 Apr 2024

Publication series

NameAIP Conference Proceedings
PublisherAmerican Institute of Physics Publising LLC
Number1
Volume3300
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference5th International Conference on Material Science and Applications, ICMSA 2024
Country/TerritoryIndia
CityAriyalur
Period10/04/2411/04/24

Keywords

  • biomaterial
  • scanning electron microscopy
  • transmission electron microscopy

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