Preparation, X-ray structure and propylaminolysis of 7,7-dichloro-5,7- dihydro-thieno[3,4-b]pyridin-5-one

Theodorus Van Es, Benjamin Staskun*, Manuel A. Fernandes

*Corresponding author for this work

    Research output: Contribution to journalArticlepeer-review

    1 Citation (Scopus)

    Abstract

    Refluxing 2-methylpyridine-3-carboxylic acid with thionyl chloride for 6-7 h gave (∼50%) title compound dichlorothienolactone 2 as was confirmed by a X-ray structure analysis. The propylaminolysis of 2 provides a new and convenient access to highly functionalised pyrrolo[3,4-b]pyridine derivatives.

    Original languageEnglish
    Pages (from-to)373-376
    Number of pages4
    JournalJournal of Chemical Research
    Issue number6
    DOIs
    Publication statusPublished - Jun 2007

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