Real-time in situ X-ray diffraction of intercalation reactions

Simon M. Clark, John S O Evans, Dermot O'Hare*, Chris J. Nuttall, Heng Vee Wong

*Corresponding author for this work

Research output: Contribution to journalArticle

30 Citations (Scopus)

Abstract

Real-time in situ energy dispersive X-ray powder diffraction techniques have been developed to monitor the intercalation of a guest species into a solid host; the time dependence of the extent of reaction (α) for the intercalation of cobaltocene CoCp2 (Cp = η5-C 5H5) by SnS2 has been experimentally determined and is consistent with a model involving nucleation followed by two-dimensional diffusion of the metallocene molecules into the host lattice.

Original languageEnglish
Pages (from-to)809-810
Number of pages2
JournalJournal of the Chemical Society, Chemical Communications
Issue number7
DOIs
Publication statusPublished - 1994
Externally publishedYes

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