Synthesis of novel bis(amides) by means of triphenyl phosphite intermediates

D. J. Barnes, R. L. Chapman, R. S. Vagg*, E. C. Watton

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

136 Citations (Scopus)

Abstract

The synthesis, via a triphenyl phosphite intermediate, of a series of bis(amides) of pyridine-2-carboxylic acid and various diamines is reported. Products isolated are of the form (C5H5NCO)2R where R = (I) -NH(CH2)2NH-, (II) -NH(CH2)3NH-, (III) -NHCH(CH2)4CHNH-, (IV) -NH(O-C6H4)NH-, and (V) H2CN(CH2)2NCH2. The compounds were characterized by microanalysis, melting point, and NMR, IR, and mass spectral data.

Original languageEnglish
Pages (from-to)349-350
Number of pages2
JournalJournal of Chemical and Engineering Data
Volume23
Issue number4
Publication statusPublished - 1978

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