Synthesis of novel bis(amides) by means of triphenyl phosphite intermediates

D. J. Barnes; R. L. Chapman; R. S. Vagg; E. C. Watton

Synthesis of novel bis(amides) by means of triphenyl phosphite intermediates

D. J. Barnes, R. L. Chapman, R. S. Vagg^*, E. C. Watton

^*Corresponding author for this work

Faculty of Science and Engineering

Research output: Contribution to journal › Article › peer-review

143 Citations (Scopus)

Abstract

The synthesis, via a triphenyl phosphite intermediate, of a series of bis(amides) of pyridine-2-carboxylic acid and various diamines is reported. Products isolated are of the form (C₅H₅NCO)₂R where R = (I) -NH(CH₂)₂NH-, (II) -NH(CH₂)₃NH-, (III) -NHCH(CH₂)₄CHNH-, (IV) -NH(O-C₆H₄)NH-, and (V) H₂CN(CH₂)₂NCH₂. The compounds were characterized by microanalysis, melting point, and NMR, IR, and mass spectral data.

Original language	English
Pages (from-to)	349-350
Number of pages	2
Journal	Journal of Chemical and Engineering Data
Volume	23
Issue number	4
Publication status	Published - 1978

Cite this

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title = "Synthesis of novel bis(amides) by means of triphenyl phosphite intermediates",

abstract = "The synthesis, via a triphenyl phosphite intermediate, of a series of bis(amides) of pyridine-2-carboxylic acid and various diamines is reported. Products isolated are of the form (C5H5NCO)2R where R = (I) -NH(CH2)2NH-, (II) -NH(CH2)3NH-, (III) -NHCH(CH2)4CHNH-, (IV) -NH(O-C6H4)NH-, and (V) H2CN(CH2)2NCH2. The compounds were characterized by microanalysis, melting point, and NMR, IR, and mass spectral data.",

author = "Barnes, \{D. J.\} and Chapman, \{R. L.\} and Vagg, \{R. S.\} and Watton, \{E. C.\}",

year = "1978",

language = "English",

volume = "23",

pages = "349--350",

journal = "Journal of Chemical and Engineering Data",

issn = "0021-9568",

publisher = "American Chemical Society",

number = "4",

}

TY - JOUR

T1 - Synthesis of novel bis(amides) by means of triphenyl phosphite intermediates

AU - Barnes, D. J.

AU - Chapman, R. L.

AU - Vagg, R. S.

AU - Watton, E. C.

PY - 1978

Y1 - 1978

N2 - The synthesis, via a triphenyl phosphite intermediate, of a series of bis(amides) of pyridine-2-carboxylic acid and various diamines is reported. Products isolated are of the form (C5H5NCO)2R where R = (I) -NH(CH2)2NH-, (II) -NH(CH2)3NH-, (III) -NHCH(CH2)4CHNH-, (IV) -NH(O-C6H4)NH-, and (V) H2CN(CH2)2NCH2. The compounds were characterized by microanalysis, melting point, and NMR, IR, and mass spectral data.

AB - The synthesis, via a triphenyl phosphite intermediate, of a series of bis(amides) of pyridine-2-carboxylic acid and various diamines is reported. Products isolated are of the form (C5H5NCO)2R where R = (I) -NH(CH2)2NH-, (II) -NH(CH2)3NH-, (III) -NHCH(CH2)4CHNH-, (IV) -NH(O-C6H4)NH-, and (V) H2CN(CH2)2NCH2. The compounds were characterized by microanalysis, melting point, and NMR, IR, and mass spectral data.

UR - https://www.scopus.com/pages/publications/0000054467

M3 - Article

AN - SCOPUS:0000054467

SN - 0021-9568

VL - 23

SP - 349

EP - 350

JO - Journal of Chemical and Engineering Data

JF - Journal of Chemical and Engineering Data

IS - 4

ER -

Synthesis of novel bis(amides) by means of triphenyl phosphite intermediates

Abstract

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